6A9V
Crystal structure of Icp55 from Saccharomyces cerevisiae (N-terminal 42 residues deletion)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | RRCAT INDUS-2 BEAMLINE PX-BL21 |
Synchrotron site | RRCAT INDUS-2 |
Beamline | PX-BL21 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2017-02-17 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 0.97947 |
Spacegroup name | I 4 2 2 |
Unit cell lengths | 142.081, 142.081, 118.731 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.554 - 2.900 |
R-factor | 0.2137 |
Rwork | 0.213 |
R-free | 0.22510 |
RMSD bond length | 0.002 |
RMSD bond angle | 0.460 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.12_2829)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.554 | 3.080 |
High resolution limit [Å] | 2.900 | 2.900 |
Rmerge | 0.157 | 1.060 |
Rmeas | 0.166 | 1.125 |
Rpim | 0.056 | 0.374 |
Number of reflections | 13770 | 2173 |
<I/σ(I)> | 15.2 | 2.5 |
Completeness [%] | 100.0 | 100 |
Redundancy | 8.7 | 8.9 |
CC(1/2) | 0.997 | 0.775 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | MICROBATCH | 7.5 | 293 | 100mM HEPES pH 7.5, 22 % Peg3350 , 250mM Ammonium Sulphate, 0.2mM MnCl2 |