6A66

Placental protein 13/galectin-13 variant R53H with Tris

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-07-01
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.98
Spacegroup name	C 2 2 2
Unit cell lengths	58.231, 92.060, 50.682
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	19.115 - 1.400
R-factor	0.1848
Rwork	0.184
R-free	0.19490
Structure solution method	MOLECULAR REPLACEMENT
Refinement software	PHENIX ((1.10.1_2155: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	19.115	1.420
High resolution limit [Å]	1.400	1.400
Number of reflections	27115
<I/σ(I)>	12.1
Completeness [%]	99.7
Redundancy	6.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	PEG