6A64

Placental protein 13/galectin-13 variant R53HR55NH57RD33G with Lactose

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL18U1
Synchrotron site	SSRF
Beamline	BL18U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-12-23
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.977
Spacegroup name	C 2 2 2
Unit cell lengths	57.351, 92.583, 50.307
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	18.910 - 1.630
R-factor	0.174
Rwork	0.170
R-free	0.20660
Structure solution method	MOLECULAR REPLACEMENT
Refinement software	PHENIX ((1.10.1_2155: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	18.910	1.660
High resolution limit [Å]	1.630	1.630
Number of reflections	17066
<I/σ(I)>	22.5
Completeness [%]	99.9
Redundancy	6.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	PEG