5ZZ3
Crystal structure of intracellular B30.2 domain of BTN3A3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-01-08 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.9793 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 50.308, 50.308, 261.093 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 3.000 |
R-factor | 0.199 |
Rwork | 0.195 |
R-free | 0.27500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4n7u |
RMSD bond length | 0.015 |
RMSD bond angle | 1.909 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0103) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.050 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.654 | |
Number of reflections | 7487 | 334 |
<I/σ(I)> | 46.625 | |
Completeness [%] | 100.0 | 100 |
Redundancy | 23.6 | |
CC(1/2) | 0.994 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | SODIUM CITRATE, IMIDAZOLE PH 8.0, 1 -PROPANOL., VAPOR DIFFUSION, SITTING DROP, TEMPERATURE 291K |