5ZXN
Crystal structure of CurA from Vibrio vulnificus
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
| Synchrotron site | Australian Synchrotron |
| Beamline | MX2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2011-08-20 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.9791 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 90.516, 91.555, 104.792 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 19.916 - 1.855 |
| R-factor | 0.2102 |
| Rwork | 0.209 |
| R-free | 0.23610 |
| Structure solution method | SAD |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.085 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Phasing software | PHENIX |
| Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 19.916 | 1.960 |
| High resolution limit [Å] | 1.855 | 1.855 |
| Rmeas | 0.117 | 1.621 |
| Number of reflections | 73918 | 10339 |
| <I/σ(I)> | 12.5 | 1.6 |
| Completeness [%] | 99.4 | 96.5 |
| Redundancy | 14.2 | 11.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | MICROBATCH | 295 | sodium chloride, MES, PEG 8000 |
