5ZW5

Structure of SeMet-spAimR

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-07-11
Detector	DECTRIS PILATUS3 R 1M
Wavelength(s)	0.97776
Spacegroup name	P 21 21 21
Unit cell lengths	33.275, 124.710, 207.063
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	47.811 - 2.400
R-factor	0.2236
Rwork	0.222
R-free	0.24790
RMSD bond length	0.003
RMSD bond angle	0.771
Data scaling software	HKL-3000
Phasing software	PHENIX
Refinement software	PHENIX ((1.11.1_2575))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.486
High resolution limit [Å]	2.400	2.400
Number of reflections	34984
<I/σ(I)>	3.16
Completeness [%]	99.9
Redundancy	11.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	0.2 M CaAc2, 20% PE G3350