5ZVV
Structure of SeMet-phAimR
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-09-10 |
Detector | DECTRIS PILATUS3 R 1M |
Wavelength(s) | 0.97776 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 61.469, 116.917, 68.244 |
Unit cell angles | 90.00, 113.55, 90.00 |
Refinement procedure
Resolution | 53.934 - 2.200 |
R-factor | 0.2106 |
Rwork | 0.208 |
R-free | 0.25130 |
RMSD bond length | 0.002 |
RMSD bond angle | 0.456 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 53.934 | 2.279 |
High resolution limit [Å] | 2.200 | 2.200 |
Number of reflections | 44287 | |
<I/σ(I)> | 3.08 | |
Completeness [%] | 98.8 | |
Redundancy | 7.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 2% Tacsimate pH 6.0, 0.1 M Bis-Tris pH 6.5, 20% PEG 3350 |