5ZV9
P domain of GII.13 norovirus capsid
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2016-12-22 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 66.688, 82.172, 115.920 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 1.800 |
R-factor | 0.16664 |
Rwork | 0.164 |
R-free | 0.21626 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4rlz |
RMSD bond length | 0.006 |
RMSD bond angle | 1.053 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.830 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.085 | 0.560 |
Number of reflections | 59172 | 2893 |
<I/σ(I)> | 25.3 | 5.4 |
Completeness [%] | 99.6 | 99.3 |
Redundancy | 6.2 | 6.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1M succinic acid (pH 7.0), 15% (w/v) polyethylene glycol (PEG) 3350 |