5ZUI
Crystal Structure of HSP104 from Chaetomium thermophilum
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-5A |
Synchrotron site | Photon Factory |
Beamline | BL-5A |
Temperature [K] | 95 |
Detector technology | CCD |
Collection date | 2015-06-10 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.0000 |
Spacegroup name | P 65 |
格子定数 [Å] | 131.182, 131.182, 137.042 |
格子定数 [度] | 90.00, 90.00, 120.00 |
精密化法
残基 | 47.382 - 2.701 |
R因子 | 0.214 |
Rwork | 0.211 |
R-free | 0.26500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4ciu |
結合角の平均二乗偏差(RMSD) [度] | 0.770 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.13_2998: ???)) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 50.000 | 2.800 |
分解能 [Å] (高) | 2.700 | 2.700 |
独立反射数 | 36348 | |
<I/σ(I)> | 31.6 | 1.2 |
完全性 [%] | 99.1 | 93.1 |
冗長性 | 10.1 | 5.1 |
CC(1/2) | 0.998 | 0.591 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 293 | 0.01 M Cobalt chloride, 0.1 M MES (pH6.5), 1.8 M Ammonium sulfate |