5ZT3
Crystal structure of WA352 from Oryza sativa
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-01-09 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9795 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 33.849, 35.435, 95.524 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.458 - 1.304 |
R-factor | 0.1881 |
Rwork | 0.188 |
R-free | 0.19320 |
Structure solution method | SAD |
RMSD bond length | 0.005 |
RMSD bond angle | 0.735 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SHELXCD |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.330 |
High resolution limit [Å] | 1.300 | 1.300 |
Number of reflections | 192774 | |
<I/σ(I)> | 12.1 | |
Completeness [%] | 98.4 | |
Redundancy | 6.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291.15 | PEG 3000, Calcium acetate, Tris base/ Hydrochloric acid |