Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

5ZRF

Crystal structure of human topoisomerase II beta in complex with 5-iodouridine-containing-DNA and etoposide in space group p21

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsNSRRC BEAMLINE BL15A1
Synchrotron siteNSRRC
BeamlineBL15A1
Temperature [K]100
Detector technologyCCD
Collection date2016-05-17
DetectorRAYONIX MX300HE
Wavelength(s)1
Spacegroup nameP 1 21 1
Unit cell lengths80.147, 176.270, 94.331
Unit cell angles90.00, 111.44, 90.00
Refinement procedure
Resolution19.869 - 2.300
R-factor0.1894
Rwork0.189
R-free0.22650
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3qx3
RMSD bond length0.006
RMSD bond angle0.863
Data scaling softwareHKL-2000
Phasing softwarePHENIX
Refinement softwarePHENIX ((1.10.1_2155: ???))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]20.0002.380
High resolution limit [Å]2.3002.300
Number of reflections99792
<I/σ(I)>18.4
Completeness [%]92.2
Redundancy2.9
CC(1/2)0.9300.738
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP277Magnesium Acetate, 2-(N-morpholino)ethanesulfonic, 2-methyl-2,4-pentanediol

225158

건을2024-09-18부터공개중

PDB statisticsPDBj update infoContact PDBjnumon