5ZKT
Crystal structure of TCP domain of PCF6 in Oryza sativa
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-05-01 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.979 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 42.280, 43.710, 72.370 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.415 - 1.740 |
R-factor | 0.2091 |
Rwork | 0.208 |
R-free | 0.21980 |
Structure solution method | SAD |
RMSD bond length | 0.006 |
RMSD bond angle | 0.653 |
Data reduction software | XDS |
Data scaling software | Aimless (0.5.32) |
Phasing software | PHENIX (1.11.1_2575) |
Refinement software | PHENIX (1.11.1_2575) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 72.370 | 72.370 | 1.790 |
High resolution limit [Å] | 1.740 | 7.780 | 1.740 |
Rmerge | 0.057 | 0.046 | 0.607 |
Rmeas | 0.059 | 0.049 | 0.630 |
Rpim | 0.016 | 0.016 | 0.166 |
Total number of observations | 196470 | 1030 | 13415 |
Number of reflections | 13997 | 138 | 970 |
<I/σ(I)> | 27.7 | 35.2 | 4.5 |
Completeness [%] | 98.0 | 63.7 | 94.8 |
Redundancy | 14 | 7.5 | 13.8 |
CC(1/2) | 0.999 | 0.997 | 0.949 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 289 | 0.2 M Ammonium sulfate, 0.1 M Sodium acetate pH4.6, 30% (w/v) PEG1500 |