5ZKF
Crystal Structure of N-terminal Domain of Plasmodium vivax p43 in space group P21
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-05-05 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9763 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 53.181, 86.942, 78.411 |
Unit cell angles | 90.00, 91.81, 90.00 |
Refinement procedure
Resolution | 43.360 - 2.750 |
R-factor | 0.221 |
Rwork | 0.215 |
R-free | 0.27850 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.160 |
Data reduction software | DIALS |
Data scaling software | xia2 |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.350 | 2.800 |
High resolution limit [Å] | 2.748 | 2.750 |
Number of reflections | 18633 | 844 |
<I/σ(I)> | 5.4 | 0.9 |
Completeness [%] | 99.5 | 89.8 |
Redundancy | 6.4 | 5.3 |
CC(1/2) | 1.000 | 0.400 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.2M sodium citrate, 20 % w/v PEG 3350 |