5ZES
UDP Glucose alpha tetrahydrobiopterin glycosyltransferase from Synechococcus species PCC 7942 - UDP complex
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 5C (4A) |
Synchrotron site | PAL/PLS |
Beamline | 5C (4A) |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-04-20 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.979,0.979,0.987 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 171.810, 78.698, 53.605 |
Unit cell angles | 90.00, 90.87, 90.00 |
Refinement procedure
Resolution | 29.010 - 2.030 |
R-factor | 0.1854 |
Rwork | 0.183 |
R-free | 0.23536 |
Structure solution method | MAD |
RMSD bond length | 0.017 |
RMSD bond angle | 1.925 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.070 |
High resolution limit [Å] | 2.030 | 2.030 |
Number of reflections | 46172 | |
<I/σ(I)> | 10 | |
Completeness [%] | 99.9 | |
Redundancy | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | Bis-tris, PEG3350, Galactose |