5ZCX
Structure of T20/N39
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-07-09 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9796 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 39.790, 38.001, 73.080 |
Unit cell angles | 90.00, 101.52, 90.00 |
Refinement procedure
Resolution | 37.535 - 2.299 |
R-factor | 0.2337 |
Rwork | 0.233 |
R-free | 0.24860 |
RMSD bond length | 0.010 |
RMSD bond angle | 0.910 |
Data scaling software | XDS |
Refinement software | PHENIX ((1.10.1_2155)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 2.381 |
High resolution limit [Å] | 2.299 | 2.299 |
Number of reflections | 9725 | |
<I/σ(I)> | 4.51 | |
Completeness [%] | 100.0 | |
Redundancy | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 291.15 | 0.05 M caesium chloride 0.1 M MES pH 6.5 30 % v/v Jeffamine M-600 |