5ZBK
Crystal structure of type-I LOG from Pseudomonas aeruginosa PAO1 in complex with AMP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 7A (6B, 6C1) |
Synchrotron site | PAL/PLS |
Beamline | 7A (6B, 6C1) |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-06-23 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 0.97934 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 64.844, 97.524, 71.788 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 54.000 - 2.300 |
R-factor | 0.1847 |
Rwork | 0.182 |
R-free | 0.23770 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5its |
RMSD bond length | 0.014 |
RMSD bond angle | 1.780 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0189) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 54.000 | 2.340 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.123 | 0.349 |
Rpim | 0.063 | 0.162 |
Number of reflections | 10160 | 493 |
<I/σ(I)> | 12.8 | |
Completeness [%] | 97.3 | |
Redundancy | 4.3 | |
CC(1/2) | 0.912 | 0.713 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.8 | 293 | ammonium phosphate dibasic, citrate pH 5.5, sodium chloride |