5ZBJ
Crystal structure of type-I LOG from Pseudomonas aeruginosa PAO1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 7A (6B, 6C1) |
Synchrotron site | PAL/PLS |
Beamline | 7A (6B, 6C1) |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-02-28 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 0.97934 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 64.931, 97.917, 71.665 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 54.110 - 1.890 |
R-factor | 0.1541 |
Rwork | 0.152 |
R-free | 0.20330 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5its |
RMSD bond length | 0.018 |
RMSD bond angle | 1.839 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 54.110 | 1.930 |
High resolution limit [Å] | 1.890 | 1.890 |
Rmerge | 0.072 | 0.347 |
Rpim | 0.036 | 0.158 |
Number of reflections | 18128 | 845 |
<I/σ(I)> | 4.5 | |
Completeness [%] | 98.1 | |
Redundancy | 5 | |
CC(1/2) | 0.804 | 0.944 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.8 | 293 | ammonium phosphate dibasic, imidazole pH 8.0 |