5ZBB
Crystal structure of Rtt109-Asf1-H3-H4 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-05-07 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9788 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 112.251, 112.251, 333.057 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 3.730 |
High resolution limit [Å] | 3.600 | 7.750 | 3.600 |
Rmerge | 0.249 | 0.055 | 0.831 |
Rmeas | 0.256 | 0.057 | 0.853 |
Rpim | 0.058 | 0.013 | 0.195 |
Number of reflections | 15314 | 1728 | 1475 |
<I/σ(I)> | 3.7 | ||
Completeness [%] | 99.9 | 99.5 | 99.9 |
Redundancy | 18.9 | 18.1 | 19.1 |
CC(1/2) | 0.999 | 0.938 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5 | 277 | 100mM sodium citrate, pH 5.0, 22% PEG 1500, 400mM sodium iodide |