5ZB5
The structural basis of histone chaperoneVps75
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BSRF BEAMLINE 3W1A |
Synchrotron site | BSRF |
Beamline | 3W1A |
Temperature [K] | 300 |
Detector technology | CCD |
Collection date | 2014-07-23 |
Detector | RIGAKU |
Wavelength(s) | 1.000 |
Spacegroup name | P 41 |
Unit cell lengths | 66.410, 66.410, 99.417 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.959 - 2.299 |
R-factor | 0.1835 |
Rwork | 0.180 |
R-free | 0.24440 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5yps |
RMSD bond length | 0.009 |
RMSD bond angle | 1.201 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.350 |
High resolution limit [Å] | 2.299 | 2.299 |
Number of reflections | 19190 | |
<I/σ(I)> | 37.1 | |
Completeness [%] | 100.0 | |
Redundancy | 7.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 289 | 0.1M Bis-Tris Propane (pH =7.0) and 20M Ammonium citrate tribasic |