5Z7G
Crystal structure of TAX1BP1 SKICH region in complex with NAP1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-03-05 |
Detector | AGILENT ATLAS CCD |
Wavelength(s) | 0.97900 |
Spacegroup name | P 63 |
Unit cell lengths | 118.487, 118.487, 64.344 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 29.622 - 2.301 |
R-factor | 0.1891 |
Rwork | 0.187 |
R-free | 0.23320 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5z7a |
RMSD bond length | 0.008 |
RMSD bond angle | 0.853 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.14_3260: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.340 |
High resolution limit [Å] | 2.300 | 2.300 |
Number of reflections | 22896 | |
<I/σ(I)> | 36.33 | |
Completeness [%] | 99.5 | 100 |
Redundancy | 19.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 289 | PEG 8000, 0.1 M HEPES |