Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

5Z6O

Crystal structure of Penicillium cyclopium protease

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU RU200
Temperature [K]290
Detector technologyAREA DETECTOR
Collection date1995-04-01
DetectorUCSD MARK II
Wavelength(s)1.54
Spacegroup nameP 21 21 21
Unit cell lengths59.223, 61.642, 70.862
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution22.721 - 1.700
R-factor0.1441
Rwork0.142
R-free0.18090
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2prk
RMSD bond length0.011
RMSD bond angle1.073
Data reduction softwareUCSD-system
Data scaling softwareAimless
Phasing softwareX-PLOR
Refinement softwarePHENIX ((1.12_2829))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]25.0001.630
High resolution limit [Å]1.6001.600
Rmerge0.0880.362
Number of reflections339851580
<I/σ(I)>10.62.8
Completeness [%]97.592.7
Redundancy5.33.3
CC(1/2)0.9960.544
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP29815% PEG 4000

226707

PDB entries from 2024-10-30

PDB statisticsPDBj update infoContact PDBjnumon