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5Z5P

Crystal structure of ConA-R3M

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSSRF BEAMLINE BL17U1
Synchrotron siteSSRF
BeamlineBL17U1
Temperature [K]100
Detector technologyCCD
Collection date2015-10-07
DetectorADSC QUANTUM 315r
Wavelength(s)0.9716
Spacegroup nameP 2 21 21
Unit cell lengths58.742, 61.945, 115.960
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution58.740 - 1.400
R-factor0.19492
Rwork0.193
R-free0.24149
RMSD bond length0.025
RMSD bond angle2.647
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHASER
Refinement softwareREFMAC (5.8.0131)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]59.0001.420
High resolution limit [Å]1.4001.400
Number of reflections84005
<I/σ(I)>2.2
Completeness [%]99.7
Redundancy12.4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP7.230020% polyethylene glycol 6000, 20 mM HEPES, 100 mM NaCl, 5 mM CaCl2, 5 mM MnCl2 pH 7.2

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