5Z4T
Complex structure - AxMan113A-M3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-06-12 |
Detector | RAYONIX MX225-HS |
Wavelength(s) | 0.979 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 65.095, 69.918, 186.601 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 32.920 - 1.680 |
R-factor | 0.1854 |
Rwork | 0.185 |
R-free | 0.21040 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5ylh |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX (dev-2474) |
Refinement software | PHENIX (dev-2474) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 32.920 | 1.740 |
High resolution limit [Å] | 1.680 | 1.680 |
Rmerge | 0.198 | |
Number of reflections | 91072 | 91702 |
<I/σ(I)> | 6.8 | |
Completeness [%] | 93.0 | 93 |
Redundancy | 9.3 | |
CC(1/2) | 0.976 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | HEPES sodium pH 7.5, 2-Propanol, PEG 4000 |