Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PAL/PLS BEAMLINE 6B |
| Synchrotron site | PAL/PLS |
| Beamline | 6B |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2004-11-12 |
| Detector | Bruker AXIOM 200 |
| Wavelength(s) | 1.12714 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 97.372, 91.289, 109.381 |
| Unit cell angles | 90.00, 113.34, 90.00 |
Refinement procedure
| Resolution | 24.308 - 1.994 |
| R-factor | 0.1843 |
| Rwork | 0.182 |
| R-free | 0.22140 |
| RMSD bond length | 0.004 |
| RMSD bond angle | 0.905 |
| Data reduction software | DENZO |
| Data scaling software | HKL-2000 |
| Phasing software | MOLREP |
| Refinement software | PHENIX (1.9_1690) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 2.070 |
| High resolution limit [Å] | 1.990 | 1.990 |
| Number of reflections | 57456 | |
| <I/σ(I)> | 44.7 | |
| Completeness [%] | 96.2 | |
| Redundancy | 6.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 294.15 | 0.1M sodium citrate pH 5.5,16% PEG 4000 , 20% isopropanol |
