5YYE
DNA polymerase IV - ternary complex 16
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-09-18 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.97264 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 86.300, 56.950, 110.710 |
Unit cell angles | 90.00, 94.79, 90.00 |
Refinement procedure
Resolution | 65.236 - 2.325 |
R-factor | 0.2031 |
Rwork | 0.200 |
R-free | 0.25510 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4ir1 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.105 |
Data reduction software | iMOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 86.000 | 2.450 |
High resolution limit [Å] | 2.325 | 2.330 |
Number of reflections | 46597 | 6752 |
<I/σ(I)> | 9 | 2 |
Completeness [%] | 99.6 | 99.8 |
Redundancy | 3.6 | 3.7 |
CC(1/2) | 0.998 | 0.674 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.2 | 298 | 15% MPD , pH 5.2, VAPOR DIFFUSION, HANGING DROP, temperature 298K |