5YY6
Crystal structure of Arabidopsis thaliana HPPD truncated mutant complexed with Benquitrione
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-05-25 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97775 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 77.333, 83.883, 66.310 |
Unit cell angles | 90.00, 100.17, 90.00 |
Refinement procedure
Resolution | 45.722 - 2.401 |
R-factor | 0.1924 |
Rwork | 0.190 |
R-free | 0.24380 |
RMSD bond length | 0.005 |
RMSD bond angle | 0.734 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.487 |
High resolution limit [Å] | 2.401 | 2.401 |
Number of reflections | 15659 | |
<I/σ(I)> | 19.76 | |
Completeness [%] | 96.0 | |
Redundancy | 2.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291.16 | PEG 400, sodium chloride, Sodium acetate |