5YWM
Crystal structure of CK2a2 form-1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL44XU |
Synchrotron site | SPring-8 |
Beamline | BL44XU |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-11-21 |
Detector | RAYONIX MX-300 |
Wavelength(s) | 0.98 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 67.292, 101.023, 45.764 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.764 - 1.939 |
R-factor | 0.1952 |
Rwork | 0.191 |
R-free | 0.24350 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3e3b |
RMSD bond length | 0.008 |
RMSD bond angle | 1.096 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.060 |
High resolution limit [Å] | 1.939 | 1.939 |
Rmerge | 0.083 | 0.637 |
Number of reflections | 44654 | |
<I/σ(I)> | 11.97 | |
Completeness [%] | 99.8 | 99.5 |
Redundancy | 5.7 | 5.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 277 | PEG 4000, Lithium sulfate monohydrate |