5YVL
Crystal structure of a cyclase Hpiu5 from Fischerella sp. ATCC 43239
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSRRC BEAMLINE BL15A1 |
Synchrotron site | NSRRC |
Beamline | BL15A1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-11-15 |
Detector | RAYONIX MX-300 |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 62.390, 114.311, 132.439 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 24.993 - 2.059 |
R-factor | 0.1809 |
Rwork | 0.179 |
R-free | 0.23610 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5yvk |
RMSD bond length | 0.014 |
RMSD bond angle | 1.497 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 25.000 | 25.000 | 2.130 |
High resolution limit [Å] | 2.059 | 4.430 | 2.060 |
Rmerge | 0.046 | 0.018 | 0.483 |
Rmeas | 0.053 | 0.020 | 0.566 |
Rpim | 0.024 | 0.009 | 0.288 |
Number of reflections | 56433 | 6233 | 5508 |
<I/σ(I)> | 16 | ||
Completeness [%] | 95.0 | 99.6 | 94.1 |
Redundancy | 4.1 | 4.6 | 3.6 |
CC(1/2) | 1.000 | 0.831 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 295 | 0.2M sodium chloride, 20%(w/v) PEG4000 |