5YUH

AtVAL1 PHD-Like domain in the P6122 space group

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-11-17
Detector	DECTRIS PILATUS3 S 6M
Wavelength(s)	0.97737
Spacegroup name	P 61 2 2
Unit cell lengths	52.743, 52.743, 125.030
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	26.371 - 1.801
R-factor	0.2473
Rwork	0.246
R-free	0.27820
Structure solution method	SAD
RMSD bond length	0.008
RMSD bond angle	0.888
Data reduction software	HKL-3000
Data scaling software	HKL-3000
Phasing software	SHELXCD
Refinement software	PHENIX ((1.10.1_2155: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	30.000	1.860
High resolution limit [Å]	1.800	1.800
Rmerge	0.094
Number of reflections	10206
<I/σ(I)>	48.25
Completeness [%]	99.9
Redundancy	33.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	0.15M DL-Malic acid pH 7.0, 20% w/v Polyethylene glycol 3350