5YSJ

SdeA mART-C domain WT apo

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SPRING-8 BEAMLINE BL44XU
Synchrotron site	SPring-8
Beamline	BL44XU
Temperature [K]	193
Detector technology	CCD
Collection date	2016-09-28
Detector	Bruker DIP-6040
Wavelength(s)	0.9
Spacegroup name	P 1 21 1
Unit cell lengths	43.962, 86.682, 71.027
Unit cell angles	90.00, 97.90, 90.00

Refinement procedure

Resolution	43.540 - 2.059
R-factor	0.2281
Rwork	0.225
R-free	0.26940
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.003
RMSD bond angle	0.725
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHENIX
Refinement software	PHENIX ((1.11.1_2575: ???))

Data quality characteristics

	Overall
Low resolution limit [Å]	43.540
High resolution limit [Å]	2.059
Number of reflections	32455
<I/σ(I)>	16.53
Completeness [%]	99.0
Redundancy	4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	PEG400, Tris