5YRK
Crystal structure of PPL3C
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL38B1 |
Synchrotron site | SPring-8 |
Beamline | BL38B1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-12-01 |
Detector | DECTRIS EIGER X 4M |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 40.250, 73.790, 90.500 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.723 - 1.350 |
R-factor | 0.1806 |
Rwork | 0.179 |
R-free | 0.20580 |
Structure solution method | SIRAS |
RMSD bond length | 0.008 |
RMSD bond angle | 1.128 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.420 |
High resolution limit [Å] | 1.350 | 1.350 |
Rmerge | 0.018 | 0.079 |
Number of reflections | 60077 | 8669 |
<I/σ(I)> | 45 | 10.2 |
Completeness [%] | 100.0 | 100 |
Redundancy | 2.4 | 2.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | 0.2M ammonium sulfate, 25%(w/v) PEG3350, 0.1M bis-Tris buffer pH 5.5 |