5YP5
Crystal structure of RORgamma complexed with SRC2 and compound 5d
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 90 |
Detector technology | CCD |
Collection date | 2011-07-13 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9792 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 62.069, 62.069, 154.818 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 57.610 - 2.650 |
R-factor | 0.20822 |
Rwork | 0.206 |
R-free | 0.25324 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.040 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 57.600 | 2.718 |
High resolution limit [Å] | 2.650 | 2.650 |
Number of reflections | 8323 | |
<I/σ(I)> | 23.4 | |
Completeness [%] | 92.6 | |
Redundancy | 7.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 0.2M Ammonium Sulfate, 0.1M Bis-Tris, pH 6.5, 14% (w/v) PEG 8000 |