5YOV
Crystal structure of BRD4-BD1 bound with hjp126
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-12-17 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97923 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 32.340, 47.435, 78.926 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 26.721 - 1.451 |
R-factor | 0.1888 |
Rwork | 0.186 |
R-free | 0.23140 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.243 |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 78.719 |
High resolution limit [Å] | 1.451 |
Number of reflections | 19355 |
<I/σ(I)> | 21 |
Completeness [%] | 87.7 |
Redundancy | 5.73 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 3.6M Naformate, 10% glycerol |