5YOU
Crystal structure of BRD4-BD1 bound with hjp64
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-12-17 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97923 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 34.622, 47.598, 77.954 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.624 - 1.503 |
R-factor | 0.2098 |
Rwork | 0.208 |
R-free | 0.24820 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 0.821 |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11_2567: ???)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 47.598 |
High resolution limit [Å] | 1.503 |
Number of reflections | 18473 |
<I/σ(I)> | 17.5 |
Completeness [%] | 87.2 |
Redundancy | 5.75 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 3.6M Naformate, 10% glycerol |