5YO3
Crystal Structure of B562RIL with engineered disulfide bond V16C-A29C
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-07-15 |
Detector | MAR CCD 130 mm |
Wavelength(s) | 0.9793 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 40.328, 50.126, 94.237 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.118 - 1.700 |
R-factor | 0.1583 |
Rwork | 0.155 |
R-free | 0.18830 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1m6t |
RMSD bond length | 0.003 |
RMSD bond angle | 0.552 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((dev_2289)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.118 | 1.780 |
High resolution limit [Å] | 1.700 | 1.700 |
Number of reflections | 10312 | |
<I/σ(I)> | 55.71 | |
Completeness [%] | 95.0 | |
Redundancy | 4.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 9 | 292 | NH4(SO4), Bicine, N-octanoylsucrose |