5YM6
Crystal Structure of porcine delta coronavirus nsp9
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-09-19 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97917 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 57.969, 55.185, 69.445 |
Unit cell angles | 90.00, 90.01, 90.00 |
Refinement procedure
Resolution | 29.789 - 1.803 |
R-factor | 0.2082 |
Rwork | 0.206 |
R-free | 0.24580 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.018 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.800 |
Number of reflections | 40635 |
<I/σ(I)> | 15.71 |
Completeness [%] | 97.4 |
Redundancy | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 3.5 | 293 | 3.0 M sodium chloride, 0.1 M citric acid (pH 3.5) |