5YM0
The crystal structure of DHAD
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSRRC BEAMLINE BL13C1 |
Synchrotron site | NSRRC |
Beamline | BL13C1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-10-14 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.96422 |
Spacegroup name | P 42 21 2 |
Unit cell lengths | 135.472, 135.472, 67.963 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.900 - 1.842 |
R-factor | 0.171 |
Rwork | 0.170 |
R-free | 0.19740 |
RMSD bond length | 0.009 |
RMSD bond angle | 0.962 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10.1_2155)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.840 |
Number of reflections | 55067 |
<I/σ(I)> | 22.6 |
Completeness [%] | 99.8 |
Redundancy | 10.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 289 | 0.1M sodium acetate pH 5.5, 1.2 M ammonium sulfate |