5YLN
Zinc dependent alcohol dehydrogenase 2 from Streptococcus pneumonia - apo form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 5C (4A) |
Synchrotron site | PAL/PLS |
Beamline | 5C (4A) |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-09-13 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.28277 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 88.177, 123.245, 130.356 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.098 - 2.189 |
R-factor | 0.2064 |
Rwork | 0.205 |
R-free | 0.25370 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2nvb |
RMSD bond length | 0.008 |
RMSD bond angle | 0.871 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.098 | 2.267 |
High resolution limit [Å] | 2.189 | 2.189 |
Rmerge | 0.093 | 0.598 |
Rmeas | 0.098 | 0.625 |
Number of reflections | 73418 | 7178 |
<I/σ(I)> | 33.73 | 7.03 |
Completeness [%] | 99.0 | 98 |
Redundancy | 11.5 | 11.9 |
CC(1/2) | 0.998 | 0.954 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 295 | 50mM Tris-HCl, pH 8.0 PEG 3000 15%(v/v), 50 mM NaCl |