5YKY
Crystal Structure of Cross-Linked Tetragonal Hen Egg White Lysozyme Soaked with 10 mM Rose Bengal and 10mM H2PtCl6
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL26B1 |
Synchrotron site | SPring-8 |
Beamline | BL26B1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-04-21 |
Detector | RIGAKU JUPITER 210 |
Wavelength(s) | 1.0 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 78.458, 78.458, 36.647 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 55.480 - 1.880 |
R-factor | 0.18454 |
Rwork | 0.182 |
R-free | 0.23748 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 193l |
RMSD bond length | 0.018 |
RMSD bond angle | 1.815 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | REFMAC |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 55.480 | 1.920 |
High resolution limit [Å] | 1.880 | 1.880 |
Number of reflections | 9257 | |
<I/σ(I)> | 18.7 | 24.28 |
Completeness [%] | 99.5 | 99.86 |
Redundancy | 13.1 | 9.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.5 | 293 | 0.7M NaCl, 0.1 M acetate buffer |