5YK6

Crystal Structure of Mmm1

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 5C (4A)
Synchrotron site	PAL/PLS
Beamline	5C (4A)
Temperature [K]	100
Detector technology	PIXEL
Collection date	2016-06-25
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.97949
Spacegroup name	P 32 2 1
Unit cell lengths	125.504, 125.504, 60.875
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	41.081 - 2.800
R-factor	0.1957
Rwork	0.194
R-free	0.23490
Structure solution method	SAD
RMSD bond length	0.008
RMSD bond angle	1.387
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Refinement software	PHENIX (1.9_1692)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.850
High resolution limit [Å]	2.800	2.800
Rmerge	0.074
Number of reflections	13895
<I/σ(I)>	26.8
Completeness [%]	99.2
Redundancy	9.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		277	PEG 10000, HEPES