Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

5YJP

Human chymase in complex with 3-(ethoxyimino)-7-oxo-1,4-diazepane derivative

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU MICROMAX-002
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date2007-05-22
DetectorRIGAKU RAXIS IV++
Wavelength(s)1.54178
Spacegroup nameP 43
Unit cell lengths75.089, 75.089, 49.750
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution23.610 - 1.800
R-factor0.15658
Rwork0.155
R-free0.18525
RMSD bond length0.033
RMSD bond angle2.486
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareAMoRE
Refinement softwareREFMAC (5.8.0158)
Data quality characteristics
 Overall
Low resolution limit [Å]100.000
High resolution limit [Å]1.800
Number of reflections24820
<I/σ(I)>14.3
Completeness [%]96.3
Redundancy5.3
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6.829322% PEG8000, 5mM zinc chloride and 100mM MES buffer

227111

PDB entries from 2024-11-06

PDB statisticsPDBj update infoContact PDBjnumon