5YIS
Crystal Structure of AnkB LIR/LC3B complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-11-11 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9793 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 61.802, 66.866, 74.148 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.712 - 2.201 |
R-factor | 0.1997 |
Rwork | 0.197 |
R-free | 0.24960 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ugm |
RMSD bond length | 0.009 |
RMSD bond angle | 1.016 |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX (1.12_2829) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.240 |
High resolution limit [Å] | 2.200 | 5.970 | 2.200 |
Rmerge | 0.111 | 0.042 | 0.954 |
Rmeas | 0.122 | 0.047 | 1.040 |
Rpim | 0.048 | 0.019 | 0.407 |
Number of reflections | 16051 | 869 | 778 |
<I/σ(I)> | 8.5 | ||
Completeness [%] | 99.5 | 95.4 | 100 |
Redundancy | 6.3 | 5.8 | 6.4 |
CC(1/2) | 0.998 | 0.809 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 8.5 | 289 | 2.4 M ammonium phosphate dibasic, 0.1 M Tris buffer (pH 8.5) |