5YIQ
Crystal structure of AnkG LIR/LC3B complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-11-12 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9793 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 64.553, 64.553, 155.461 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 50.000 - 2.600 |
R-factor | 0.2194 |
Rwork | 0.217 |
R-free | 0.25890 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ugm |
RMSD bond length | 0.008 |
RMSD bond angle | 1.265 |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.640 |
High resolution limit [Å] | 2.600 | 7.050 | 2.600 |
Rmerge | 0.134 | 0.048 | 1.210 |
Rmeas | 0.149 | 0.055 | 1.338 |
Rpim | 0.064 | 0.025 | 0.563 |
Number of reflections | 6417 | 385 | 310 |
<I/σ(I)> | 7.4 | 1.9 | |
Completeness [%] | 99.7 | 96 | 100 |
Redundancy | 5.3 | 4.3 | 5.6 |
CC(1/2) | 0.998 | 0.547 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6.5 | 289 | 10% v/v 2-propanol, 0.2 M zinc acetate, 0.1 M MES buffer (pH 6.5) |