5YEL
Crystal structure of CTCF ZFs6-11-gb7CSE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-03-16 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9795 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 190.993, 69.631, 84.445 |
Unit cell angles | 90.00, 116.25, 90.00 |
Refinement procedure
Resolution | 37.874 - 2.960 |
R-factor | 0.2687 |
Rwork | 0.268 |
R-free | 0.28560 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.310 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.12_2829: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.870 | 3.010 |
High resolution limit [Å] | 2.900 | 2.960 |
Rmerge | 0.087 | 0.653 |
Rpim | 0.029 | 0.221 |
Number of reflections | 30548 | |
<I/σ(I)> | 30.6 | 4.3 |
Completeness [%] | 99.6 | 100 |
Redundancy | 9.6 | 9.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 289 | 0.1M Bis-tris pH 5.6-6.0, 0.1M Sodium chloride, 17-20% PEG3350 |