Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

5YDO

Regulatory domain of HypT from Salmonella typhimurium (apo-form)

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsPAL/PLS BEAMLINE 5C (4A)
Synchrotron sitePAL/PLS
Beamline5C (4A)
Temperature [K]100
Detector technologyCCD
Collection date2015-12-12
DetectorADSC QUANTUM 315
Wavelength(s)0.97960
Spacegroup nameP 41 21 2
Unit cell lengths63.344, 63.344, 100.807
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution39.441 - 2.000
R-factor0.2069
Rwork0.204
R-free0.25360
Structure solution methodSAD
RMSD bond length0.003
RMSD bond angle0.553
Data reduction softwareDENZO
Data scaling softwareHKL-2000
Phasing softwareAutoSol
Refinement softwarePHENIX ((1.12_2829: ???))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.030
High resolution limit [Å]2.0002.000
Rmerge0.0580.207
Rpim0.0130.061
Number of reflections14482677
<I/σ(I)>41.236.29
Completeness [%]99.395.6
Redundancy16.59.6
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6.528750mM ammonium sulfate, 50mM Bis-Tris (pH 6.5), 30%(v/v) pentaerythritol ethoxylate (15/4 EO/OH), and 2mM TCEP.

226707

PDB entries from 2024-10-30

PDB statisticsPDBj update infoContact PDBjnumon