5YB2
Crystal structure of LP-11/N44
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL17U1 |
| Synchrotron site | SSRF |
| Beamline | BL17U1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2016-11-17 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.9796 |
| Spacegroup name | H 3 |
| Unit cell lengths | 110.884, 110.884, 125.382 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 27.720 - 3.800 |
| R-factor | 0.2841 |
| Rwork | 0.283 |
| R-free | 0.30680 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Data scaling software | HKL-2000 (V1.0) |
| Phasing software | PHASER (7.0) |
| Refinement software | PHENIX (1.10.1-2155-000) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 27.720 |
| High resolution limit [Å] | 3.800 |
| Number of reflections | 5647 |
| <I/σ(I)> | 14.4 |
| Completeness [%] | 100.0 |
| Redundancy | 5.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 291.15 | 0.1 M HEPES pH 7.5, 2.0 M Ammonium sulfate |
