5YAY
Crystal structure of KANK1/KIF21A complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-04-02 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.98 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 38.043, 52.080, 136.095 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.484 - 1.550 |
R-factor | 0.1841 |
Rwork | 0.183 |
R-free | 0.19980 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4hbd |
RMSD bond length | 0.012 |
RMSD bond angle | 1.353 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.8.4_1496) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.580 |
High resolution limit [Å] | 1.550 | 4.210 | 1.550 |
Rmerge | 0.057 | 0.039 | 0.835 |
Rmeas | 0.064 | 0.044 | 0.929 |
Rpim | 0.028 | 0.021 | 0.397 |
Number of reflections | 39577 | 1798 | 2005 |
<I/σ(I)> | 15.1 | ||
Completeness [%] | 98.2 | 81 | 100 |
Redundancy | 5.4 | 4.5 | 5.5 |
CC(1/2) | 0.996 | 0.688 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 289 | 0.2 M ammonium formate and 20% w/v polyethylene glycol 3350 |