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5Y9Q

Crystal structure of the CcpE regulatory domain at 1.95 Angstrom from Staphylococcus aureus

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsPAL/PLS BEAMLINE 5C (4A)
Synchrotron sitePAL/PLS
Beamline5C (4A)
Temperature [K]100
Detector technologyCCD
Collection date2017-06-25
DetectorADSC QUANTUM 315r
Wavelength(s)0.9826
Spacegroup nameH 3
Unit cell lengths111.667, 111.667, 123.120
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution26.207 - 1.953
R-factor0.1791
Rwork0.177
R-free0.22040
Structure solution methodSAD
RMSD bond length0.014
RMSD bond angle1.378
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHENIX
Refinement softwarePHENIX (1.8.4_1496)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0001.980
High resolution limit [Å]1.9501.950
Rmerge0.1040.104
Number of reflections7583641088
<I/σ(I)>2.3
Completeness [%]99.099
Redundancy8.38.3
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP82874 M Sodium formate

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