5Y9H
Crystal structure of SafDAA-dsc complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-12-10 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 0.9793 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 133.270, 66.070, 187.680 |
Unit cell angles | 90.00, 96.22, 90.00 |
Refinement procedure
Resolution | 93.288 - 2.800 |
R-factor | 0.2205 |
Rwork | 0.219 |
R-free | 0.25480 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2IXQ and 5Y9G |
RMSD bond length | 0.006 |
RMSD bond angle | 0.993 |
Data reduction software | iMOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 93.300 | 2.950 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.140 | 1.480 |
Number of reflections | 38710 | |
<I/σ(I)> | 8.1 | |
Completeness [%] | 96.0 | 96.1 |
Redundancy | 5.9 | 6 |
CC(1/2) | 0.440 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | PEG4000 |