5Y96
Crystal structure of ANXUR1 extracellular domain from Arabidopsis thaliana
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL19U1 |
| Synchrotron site | SSRF |
| Beamline | BL19U1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2016-03-18 |
| Detector | DECTRIS PILATUS3 6M |
| Wavelength(s) | 0.9785 |
| Spacegroup name | P 1 |
| Unit cell lengths | 54.679, 68.740, 70.327 |
| Unit cell angles | 88.95, 75.00, 72.18 |
Refinement procedure
| Resolution | 43.339 - 1.800 |
| R-factor | 0.1826 |
| Rwork | 0.182 |
| R-free | 0.20400 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 5y92 |
| RMSD bond length | 0.003 |
| RMSD bond angle | 0.571 |
| Data scaling software | SCALEPACK |
| Phasing software | SOLVE |
| Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 1.800 |
| Number of reflections | 83947 |
| <I/σ(I)> | 17.3 |
| Completeness [%] | 96.5 |
| Redundancy | 3.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.2M Ammonium acetate,0.1M HEPES pH 7.5,25%(w/v) Polyethylene glycol 3,350 |
